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Thermal Chemical Vapor Deposition (TCVD) System

Versatile Platform for Advanced Nanomaterials & 2D Thin Film Growth

Blue Wave Semiconductor offers the TCVD System, a versatile platform engineered for controlled chemical vapor deposition of advanced nanomaterials such as MoS₂, WS₂, and graphene. Designed around a robust quartz tube reactor, the system accommodates multiple small substrates or wafer pieces for flexible research workflows.[cite: 2]

The TCVD System incorporates a digitally controlled high-temperature heating module capable of reaching up to 1100°C. Its vacuum-compatible quartz tube is sealed with elastomer O-rings and stainless-steel flanges, featuring integrated gas inlet/outlet hardware enabling operation under vacuum or controlled-gas environments.[cite: 2]

Replaceable quartz tube reaction chamber
3-Zone heating furnace (Up to 1200°C)
Base pressure < 5×10⁻³ Torr
Closed-loop dual pressure controllers
High-temperature ceramic substrate boat
Full computer automation & safety interlocks
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TCVD Research & Industrial Capabilities

Graphene Growth
Graphene Growth
MoS2 Growth Coatings
MoS₂ Growth Coatings
Optical Transparent Coatings
Optical Transparent Coatings
Oxide & Nitride Coatings
Oxide & Nitride Coatings
Dielectric Coatings
Dielectric Coatings (Low & High-k)
Metallic & Multilayer Thin Films
Multilayer Thin Films
Semiconductor Layer Epitaxial Growth
Semiconductor Epitaxial Layer
Corrosion & Diffusion Barrier Layers
Barrier Layers (Si₃N₄, TiN)

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Explore live demonstrations and key capabilities of our custom semiconductor deposition equipment.

HFCVD Heater Z and Rotation Stage

Blue Wave Substrate/Wafer rotation products are capable of reaching up to 700¡ÆC while rotating up to 10-20 rpm. Compatible with reactive sputtering, PLD, PVD, e-beam and thermal evaporation, PECVD, ALD, in UHV or inert and reactive gas environments.[cite: 1]

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Sputtering Process

Sputtering is a process whereby atoms are ejected from a solid target material due to bombardment of the target by energetic ions. Sputter deposition is a physical vapor deposition (PVD) method for depositing thin films onto a substrate.[cite: 1]

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HFCVD Heater Z and Rotation Stage

Blue Wave Substrate/Wafer rotation products are capable of reaching up to 700¡ÆC while rotating up to 10-20 rpm. Compatible with reactive sputtering, PLD, PVD, e-beam and thermal evaporation, PECVD, ALD, in UHV or inert and reactive gas environments.[cite: 1]

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In-Depth System Information

1 Quartz Deposition Chamber

  • Vacuum chamber equipped with a replaceable quartz tube designed to prevent cross-contamination[cite: 2]
  • Stainless steel adapters with elastomer O-rings for tight seal around quartz tube[cite: 2]
  • Conveniently removable adapters for easy quartz tube replacement and O-ring maintenance[cite: 2]
  • Quick access ports on both sides for effortless sample loading[cite: 2]
  • Precisely positioned within furnace for optimal heating efficiency and thermal exposure[cite: 2]

2 System Framework

  • Clean room-grade frame for holding furnace and system components[cite: 2]
  • Integrated rackmount mounting for electronics, power distribution, and control systems[cite: 2]
  • Equipped with mobility casters and leveling features for easy installation and adjustment[cite: 2]

3 Chamber Pumping

  • Oil mechanical pump capable of achieving high vacuum levels better than 5×10⁻³ Torr[cite: 2]
  • Includes all hardware, vacuum plumbing, and valves for pumping and venting operations[cite: 2]
  • Compact, efficient design optimized for long-term operational stability[cite: 2]

4 Oil Mechanical Pump

  • High-performance rotary vane oil pump optimized for process stability[cite: 2]
  • Equipped with an isolation valve to protect against oil back-streaming[cite: 2]

5 Gas Flow and Pressure Control

  • Ventilated enclosure housing mass flow controllers (MFCs) interfaced with facility exhaust[cite: 2]
  • Tailored selection of MFCs with built-in shut-off valves for safety and cross-contamination prevention[cite: 2]
  • Two closed-loop pressure controllers for precise regulation at low and high pressure[cite: 2]
  • Built-in pressure relief valve in ventilated gas cabinet for maximum safety[cite: 2]

6 Vacuum Gauge

  • Combination gauge integrating capacitance and Pirani measurement methods[cite: 2]
  • Digital pressure readout display included with mounting hardware and cables[cite: 2]
  • Resists metal and oxide contamination over extended use[cite: 2]

7 Furnace

  • Adjustable heating across three process zones for custom thermal profiles[cite: 2]
  • Quartz tube precisely positioned to maximize heating efficiency and maintain uniform thermal profiles[cite: 2]
  • Precise temperature controllability for consistent and repeatable thermal growth[cite: 2]
  • Clean operation designed for high-temperature processing without introducing contamination[cite: 2]

8 Substrate Boat

  • Constructed from high-temperature ceramic to ensure thermal stability[cite: 2]
  • Accommodates a range of sample sizes and substrates[cite: 2]
  • Straightforward loading/unloading operation using the provided loading rod[cite: 2]

9 System Cooling

  • Water-cooled components maintain stable operation during high-temperature processes[cite: 2]
  • Enhances overall process stability and thermal repeatability[cite: 2]
  • Connected to an integrated recirculating chiller (e.g., CW-3000)[cite: 2]

10 Computer Control & Automation

  • Gas flow control and monitoring[cite: 2]
  • Chamber pressure control and vacuum measurements[cite: 2]
  • Furnace power control and multi-zone temperature monitoring[cite: 2]
  • Adjustable safety interlocks (Water Flow, Over Pressure, O₂/H₂ Ratio, Exhaust, Temp)[cite: 2]
  • Library system for users to save and load custom recipes[cite: 2]
OP-1. Additional Gas/Mass Flow Controller

Add up to 6 additional mass flow controllers (MFCs) into the system. Gases may include Nitrogen (N₂), Argon (Ar), Methane (CH₄), Hydrogen (H₂), and various dopant gases. Contact Blue Wave for custom flow range options.[cite: 2]

OP-2. System Fume Hood

An external fume hood can be integrated to provide enhanced ventilation and safe removal of process exhaust. Fully compatible with standard laboratory ducting and exhaust systems for straightforward setup.[cite: 2]

Accessories coming soon. Contact us for compatible ceramic boats, quartz tubes, and add-ons.
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TCVD System Brochure

Download our detailed brochure for complete specifications, configuration options, and ordering information.

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Technical Specifications

Specification Parameter
Base Pressure5 × 10⁻³ Torr[cite: 2]
Operating Pressure Range1 – 760 Torr[cite: 2]
Mechanical Pump Speed17.4 m³/h[cite: 2]
Input Power208 VAC, 3 Phase, 10 Amp[cite: 2]
Substrate Temperature Range200 – 1200°C (3 Zone Controllers)[cite: 2]
Vacuum PumpOil Pump[cite: 2]
CoolingWater Cooling[cite: 2]
Vacuum SealsElastomer O-rings[cite: 2]
Deposition AreaUp to 2” Diameter[cite: 2]
Deposition CapabilitiesSingle/Bilayer/Multilayer Graphene, MoS₂[cite: 2]
Substrate HolderCeramic Boat[cite: 2]
Tube ReactorQuartz[cite: 2]
Interlock ControlWater Flow, Over Pressure, O₂/H₂ Ratio, Exhaust, Temperature[cite: 2]
System Size6 ft × 3 ft × 6 ft (L×D×H)[cite: 2]
MFCs (Customer Specified)H₂: 0–200 SCCM | CH₄: 0–2000 SCCM | Ar: 0–200 SCCM[cite: 2]

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